3-(2-甲基-1,3-二氧戊环-2-基)丙基乙酸酯合成路线 (共 3 条)
反应条件
1: LiAlH4
2: 100 percent / Et3N / CH2Cl2 / 2 h / 0 - 5 °C
3: LiBr / acetone / 1.) room temperature, overnight, 2.) reflux, 4 h
View Scheme
参考文献
Joshi, Navalkishore N.; Mamdapur, Vasant R.; Chadha, Mohindra S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2963 - 2966
反应条件
sodium hydroxide in ethanol
15 h;
参考文献
Odinokov, V. N.; Kukovinets, O. S.; Zainullin, R. A.; Ishmuratov, G. Yu.; Isakova, L. A.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 11 p. 2017 - 2021
Zhurnal Organicheskoi Khimii, 1986 , vol. 23, # 11 p. 2288 - 2293
反应条件
1: LiAlH4
2: 100 percent / Et3N / CH2Cl2 / 2 h / 0 - 5 °C
View Scheme
参考文献
Joshi, Navalkishore N.; Mamdapur, Vasant R.; Chadha, Mohindra S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2963 - 2966