1: (LGACAGL)2 With hydrogenchloride; water pH=3.5; 0.166667 h; UV-irradiationPhotolysis; 2: With hydrogenchloride; water T=115°C; 10 h; 3: (9H-Fluoren-9-yl)-methyl chloroformate in acetone; pentane
参考文献
Mozziconacci, Olivier; Kerwin, Bruce A.; Schoeneich, Christian
Journal of Physical Chemistry B, 2010 , vol. 114, # 19 p. 6751 - 6762
1.1: Fmoc-Cl; N-methylmorpholine / tetrahydrofuran / 0.17 h / -15 °C 1.2: 91 percent / tetrahydrofuran; diethyl ether / 0 - 20 °C 2.1: 78 percent / silver benzoate / dioxane; H2O / 0.02 h / microwave irradiation View Scheme
参考文献
Vasanthakumar, Ganga-Ramu; Patil, Basanagoud S.; Suresh Babu, Vommina V.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 18 p. 2087 - 2089