N-(4-氯苯基)-对甲苯磺酰胺合成路线 （共 33 条）
反应条件
1: pyridine / tetrahydrofuran / 0 - 20 °C / |Inert atmosphere
2: N-chloro-succinimide; oxygen; copper dichloride / acetonitrile / 4 h / 100 °C / 760.05 Torr
View Scheme
参考文献
Urones, Beatriz; Martinez, Angel Manu; Rodriguez, Nuria; Arrayas, Ramon Gomez; Carretero, Juan C.
Chemical Communications, 2013 , vol. 49, # 94 p. 11044 - 11046
反应条件
1,4,7,10-tetraoxa-cyclododecane; potassium tert-butylate
1) THF, r.t., 30 min, 2) r.t., 1d; Multistep reaction. Yields of byproduct given;
参考文献
Ono; Todoriki; Tamura
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 4 p. 866 - 873
反应条件
1,4,7,10-tetraoxa-cyclododecane; potassium tert-butylate
1) THF, r.t., 30 min, 2) r.t., 2d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ono; Todoriki; Tamura
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 4 p. 866 - 873
参考文献
Klamann; Bertsch
Chemische Berichte, 1956 , vol. 89, p. 2007,2011
参考文献
Suzuki, Hitomi; Takaoka, Koji
Chemistry Letters, 1984 , p. 1733 - 1736
反应条件
in acetonitrile
T=50°C; Rate constant;
参考文献
Oh, Hyuck Keun; Kwon, Young Bong; Chung, Dong Soo; Lee, Ikchoon
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 10 p. 683 - 688
反应条件
in acetonitrile
T=50°C; Rate constant;
参考文献
Oh, Hyuck Keun; Kwon, Young Bong; Chung, Dong Soo; Lee, Ikchoon
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 10 p. 683 - 688
反应条件
sodium ethanolate
T=40°C; Rate constant;
参考文献
Ono; Araya; Tamura
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 5 p. 1373 - 1378
反应条件
in butanone
T=14.85°C; Substitution; KineticsThermodynamic data; Further Variations:TemperaturesSolvents;
参考文献
Kustova; Kuritsyn
Russian Journal of General Chemistry, 2000 , vol. 70, # 3 p. 457 - 458
反应条件
in acetonitrile
5 h; Irradiation;
参考文献
Park, Kwanghee Koh; Lee, Jin Joo; Ryu, Jaegyung
Tetrahedron, 2003 , vol. 59, # 39 p. 7651 - 7659
