5-苄氧基-4-氮杂吲哚-2-羧酸合成路线 （共 6 条）
反应条件
in o-xylene T=170°C; 0.416667 h;
参考文献
Chang, Han-Ting; Charmot, Dominique; Glinka, Tomasz; Cope, Michael James; Goka, Elizabeth; Shao, Jun; Cartigny, Damien; Chen, Shiah-yun; Buysse, Jerry M.
Patent: US2007/135385 A1, 2007 ;
Location in patent: Page/Page column 120-121 ;
US 20070135385 A1
反应条件
1: 61 percent / Na / ethanol / 72 h / -15 °C 2: 67 percent / o-xylene / 0.42 h / 170 °C View Scheme
参考文献
Fresneda, Pilar M.; Molina, Pedro; Delgado, Santiago; Bleda, Juan A.
Tetrahedron Letters, 2000 , vol. 41, # 24 p. 4777 - 4780
反应条件
1: 77 percent / mesityllithium 2: 61 percent / NaOEt / ethanol / -15 °C 3: 67 percent / xylene / Heating View Scheme
参考文献
Fresneda, Pilar M.; Molina, Pedro; Delgado, Santiago; Bleda, Juan A.
Tetrahedron Letters, 2000 , vol. 41, # 24 p. 4777 - 4780
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Reduction; Heating;
参考文献
Molina, Pedro; Fresneda, Pilar M.; Delgado, Santiago
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 489 - 499
反应条件
sodium hydride in N,N-dimethyl-formamide silylation;
参考文献
Molina, Pedro; Fresneda, Pilar M.; Delgado, Santiago
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 489 - 499
反应条件
1: 93 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating 2: 60 percent / MnO2 / CH2Cl2 / 72 h / 20 °C View Scheme
参考文献
Fresneda, Pilar M.; Molina, Pedro; Delgado, Santiago; Bleda, Juan A.
Tetrahedron Letters, 2000 , vol. 41, # 24 p. 4777 - 4780
