4-甲氧基-1H-吡咯并[2,3-B]吡啶-2-甲醛合成路线 （共 5 条）
反应条件
manganese(IV) oxide in dichloromethane T=20°C; Oxidation;
参考文献
Molina, Pedro; Fresneda, Pilar M.; Delgado, Santiago
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 489 - 499
反应条件
1: 93 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating 2: 60 percent / MnO2 / CH2Cl2 / 72 h / 20 °C View Scheme
参考文献
Fresneda, Pilar M.; Molina, Pedro; Delgado, Santiago; Bleda, Juan A.
Tetrahedron Letters, 2000 , vol. 41, # 24 p. 4777 - 4780
反应条件
1: 67 percent / o-xylene / 0.42 h / 170 °C 2: 93 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating 3: 60 percent / MnO2 / CH2Cl2 / 72 h / 20 °C View Scheme
参考文献
Fresneda, Pilar M.; Molina, Pedro; Delgado, Santiago; Bleda, Juan A.
Tetrahedron Letters, 2000 , vol. 41, # 24 p. 4777 - 4780
反应条件
1: 61 percent / Na / ethanol / 72 h / -15 °C 2: 67 percent / o-xylene / 0.42 h / 170 °C 3: 93 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating 4: 60 percent / MnO2 / CH2Cl2 / 72 h / 20 °C View Scheme
参考文献
Fresneda, Pilar M.; Molina, Pedro; Delgado, Santiago; Bleda, Juan A.
Tetrahedron Letters, 2000 , vol. 41, # 24 p. 4777 - 4780
反应条件
1: 77 percent / mesityllithium 2: 61 percent / NaOEt / ethanol / -15 °C 3: 67 percent / xylene / Heating 4: 93 percent / AlLiH4 / tetrahydrofuran / Heating 5: 60 percent / MnO2 / CH2Cl2 / 20 °C View Scheme
参考文献
Fresneda, Pilar M.; Molina, Pedro; Delgado, Santiago; Bleda, Juan A.
Tetrahedron Letters, 2000 , vol. 41, # 24 p. 4777 - 4780
