2,4,6-三甲基苯甲腈N-氧化物合成路线 （共 55 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran T=0°C; 4 h; other LDA-conc.; other temp; further 1,3-dithiolan-1,1-dioxide; Product distribution;
参考文献
Chemische Berichte, , vol. 121, p. 1159 - 1164
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0°C; 2 h; other reagents and reag.-conc.; Product distribution;
参考文献
Chemische Berichte, , vol. 121, p. 1159 - 1164
反应条件
lithium diisopropyl amide 1.) 0 deg C; Multistep reaction. Yields of byproduct given;
参考文献
Schaumann, Ernst; Ruhter, Gerd
Tetrahedron Letters, 1985 , vol. 26, # 43 p. 5265 - 5268
参考文献
Schaumann, Ernst
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 11 p. 995 - 1008
反应条件
in ethanol; water T=25°C; controlled pot. electrolysis at -0.70 V, var.: solvent DMF; Mechanism;
参考文献
Kubota, Tanekazu; Hiramatsu, Sadaaki; Kano, Kenji; Uno, Bunji; Miyazaki, Hiroshi
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3830 - 3839
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran T=0°C; 4 h; other LDA-conc.; without HMPT; also with CH3I or BuLi; Product distribution;
参考文献
Chemische Berichte, , vol. 121, p. 1159 - 1164
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran T=0°C; 4 h; other LDA-conc.; other temp; further 1,3-dithiolan-1,1-dioxide; Product distribution;
参考文献
Chemische Berichte, , vol. 121, p. 1159 - 1164
反应条件
potassium tert-butylate 1) THF, 2) 3 h, 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schaumann, Ernst; Ruehter, Gerd
Chemische Berichte, 1988 , vol. 121, p. 1159 - 1164
反应条件
in benzene 24 h; Heatingother solvent, reaction time; Product distribution;
参考文献
Corsaro, Antonino; Librando, Vito; Chiacchio, Ugo; Pistara, Venerando; Rescifina, Antonio
Tetrahedron, 1998 , vol. 54, # 31 p. 9187 - 9194
反应条件
lithium diisopropyl amide multistep reaction: various reagents; Product distribution;
参考文献
Schaumann, Ernst; Ruehter, Gerd
Chemische Berichte, 1988 , vol. 121, p. 1159 - 1164
