二(2,6-二甲苯基)二硫醚合成路线 (共 17 条)
反应条件
indium; ammonium chloride in ethanol Reduction; 1 h; Heating;
参考文献
Vidya Sagar Reddy; Venkat Rao; Iyengar
Synthetic Communications, 2000 , vol. 30, # 5 p. 859 - 862
反应条件
in pentane 2 h; Ambient temperature; Yield given;
参考文献
Davis, Franklin A.; Jenkins, Robert H.; Rizvi, Syed Q. A.; Yocklovich, Steven G.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3467 - 3474
反应条件
oxygen; SiO2-Cl in dichloromethane
T=0°C; 0.166667 h;
参考文献
Sathe, Manisha; Ghorpade, Ramarao; Kaushik, Mahabir Parshad
Chemistry Letters, 2006 , vol. 35, # 9 p. 1048 - 1049
反应条件
water; copper(l) chloride in dichloromethane
T=20 - 30°C; 3 h; ultrasonic irradiation;
参考文献
Ma, Ming; Zhang, Xiu; Peng, Lingling; Wang, Jianbo
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1095 - 1097
反应条件
in diethyl ether
T=0°C; 1 h;
参考文献
Aubart, Mark A.; Bergman, Robert G.
Journal of the American Chemical Society, 1998 , vol. 120, # 34 p. 8755 - 8766
反应条件
tetra-n-butylammonium perchlorate in carbon disulfide; ethanol
T=0°C; Electrochemical reaction;
参考文献
Barba, Fructuoso; Ranz, Fernando; Batanero, Belen
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6798 - 6799
反应条件
triphenylphosphine in tetrahydrofuran
T=20°C;
参考文献
Kabalka, George W.; Reddy, Marepally Srinivasa; Yao, Min-Liang
Tetrahedron Letters, 2009 , vol. 50, # 52 p. 7340 - 7342
反应条件
propynoic acid methyl ester in toluene
T=520°C; flash vacuum pyrolysis;
参考文献
Davis, Franklin A.; Jenkins, Robert H.; Rizvi, Syed Q. A.; Yocklovich, Steven G.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3467 - 3474
反应条件
water; silica gel
20 h; Mechanism; regioselective reaction;
参考文献
Kundu, Samir; Roy, Babli; Basu, Basudeb
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 26 - 33
反应条件
copper(l) iodide; tetra(n-butyl)ammonium hydroxide; sulfur in water
T=40°C; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Xu, Hua-Jian; Liang, Yu-Feng; Cai, Zhen-Ya; Qi, Hong-Xia; Yang, Chun-Yan; Feng, Yi-Si
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 2296 - 2300