二(2,6-二甲苯基)二硫醚合成路线 （共 17 条）
反应条件
1: 90 percent / m-chloroperbenzoic acid / CHCl3 / 1.) 0 deg C, 2.) 0.5 h, room temp.
2: 15 percent / methyl propiolate / toluene / 520 °C / flash vacuum pyrolysis
View Scheme
参考文献
Davis, Franklin A.; Jenkins, Robert H.; Rizvi, Syed Q. A.; Yocklovich, Steven G.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3467 - 3474
反应条件
1: H2O / Erwaermen des Reaktionsprodukts mit LiAlH4 in Aether
2: iodine; ethanol
View Scheme
参考文献
Campaigne; Osborn
Journal of Organic Chemistry, 1957 , vol. 22, p. 561
反应条件
(i) NaNO2, aq. HCl, dioxane, (ii) SO2, CuCl2, KCl, benzene; Multistep reaction;
参考文献
Prinsen,A.J.; Cerfontain,H.
Recueil des Travaux Chimiques des Pays-Bas, 1965 , vol. 84, p. 24 - 30
反应条件
meta-chloroperoxybenzoic acid; oxygen; sodium chloride in n-heptane
Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Laan, R. van der; Moolenaar, M.J.; Koning, H. de; Huisman, H.O.
Recueil des Travaux Chimiques des Pays-Bas, 1985 , vol. 104, # 9 p. 220 - 225
反应条件
(i) aq. NaOH, EtOH, (ii) Br2; Multistep reaction;
参考文献
Cox,J.R. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1083 - 1092
反应条件
1: pentane / 2 h / Ambient temperature
2: 90 percent / m-chloroperbenzoic acid / CHCl3 / 1.) 0 deg C, 2.) 0.5 h, room temp.
3: 65 percent / methyl propiolate / toluene / 520 °C / flash vacuum pyrolysis
View Scheme
参考文献
Davis, Franklin A.; Jenkins, Robert H.; Rizvi, Syed Q. A.; Yocklovich, Steven G.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3467 - 3474
反应条件
1: (i) Cl2, (ii) /BRN= 956570/
2: 150 - 170 °C
View Scheme
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013
