1: (PhIO)n 2: 89 percent / Zn, trimethylchlorosilane / neat (no solvent) / 6 h / Ambient temperature View Scheme
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Dartiguelongue, Caroline; Payan, Steve; Duval, Olivier; Gomes, Luis M.; Waigh, Roger D.
Bulletin de la Societe Chimique de France, 1997 , vol. 134, # 8-9 p. 769 - 772
Yoshida, Kenji; Taguchi, Masahiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 919 - 922
trimethylsilyl cyanide; lithium perchlorate in benzene T=25°C; 0.75 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sundberg, Richard J.; Theret, Marie-Helene; Wright, Lorna
Organic Preparations and Procedures International, 1994 , vol. 26, # 3 p. 386 - 389
Dartiguelongue, Caroline; Payan, Steve; Duval, Olivier; Gomes, Luis M.; Waigh, Roger D.
Bulletin de la Societe Chimique de France, 1997 , vol. 134, # 8-9 p. 769 - 772
electrolysis on platinum cathode and anode in methanol; water 16 h; Ambient temperatureother aza-rings, var. time, temp., and DC-voltage; Product distribution;
in methanol; water T=20°C; Electrolysis; Product distribution; Further Variations:Temperaturestime, electrode potential, concentrations, ratios of solvent;
参考文献
Zhao, Ping; Yin, Ying-Wu
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 2 p. 157 - 160
