7,3',4'-三-O-甲基毛地黄黄酮合成路线 （共 33 条）
反应条件
1: 97 percent / K2CO3 / acetone / 2 h / Heating
2: 86 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.5 h / 0 - 20 °C
3: 96 percent / K2CO3 / acetone / 1 h / Heating
View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 97 percent / K2CO3 / acetone / 2 h / Heating
2: 86 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.5 h / 0 - 20 °C
View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 97 percent / K2CO3 / acetone / 2 h / Heating
2: 86 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.5 h / 0 - 20 °C
3: 96 percent / K2CO3 / acetone / 1 h / Heating
4: 99 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C
5: 89 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.83 h / 0 - 20 °C
View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
