2-异丙氧基-5-三氟甲氧基苯硼酸合成路线 (共 2 条)
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-30°C; 0.666667 h; 2: With triisopropyl borane in tetrahydrofuran; hexane T=-78°C; 1.08333 h; 3: With hydrogenchloride; water in tetrahydrofuran; hexane T=-78 - 20°C; 0.5 h;
参考文献
PFIZER LIMITED
Patent: WO2006/67587 A2, 2006 ;
Location in patent: Page/Page column 27 ;
反应条件
1: With Oxonereg;; sodium hydroxide; ethylenediaminetetraacetic acid; water; sodium hydrogencarbonate in acetone
T=0 - 20°C; 2.08333 h;
2: With hydrogenchloride in acetone
参考文献
PFIZER LIMITED
Patent: WO2006/67587 A2, 2006 ;
Location in patent: Page/Page column 27; 28 ;