2,2,4,4-四甲基-3-戊酮亚胺合成路线 （共 19 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; Oxidation; 1 h;
参考文献
Choong, Ingrid C.; Ellman, Jonathan A.
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6528 - 6529
反应条件
hydrogenchloride T=85 - 90°C; 6 h;
参考文献
Knorr, Rudolf; Donhaerl, Angelika; Hennig, Karsten-Olaf
Liebigs Annales, 1996 , # 2 p. 155 - 157
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol
参考文献
Bordwell; Zhang, Shizbong
Journal of the American Chemical Society, 1995 , vol. 117, # 17 p. 4858 - 4861
反应条件
triethylamine in tetrachloromethane Heating;
参考文献
Weidner, Reinhold; Wuerthwein, Ernst-Ulrich
Chemische Berichte, 1989 , vol. 122, p. 1095 - 1106
反应条件
triethylamine in toluene
14 h; Ambient temperature;
参考文献
Kupfer, Rainer; Wuerthwein, Ernst-Ulrich
Chemische Berichte, 1986 , vol. 119, # 3 p. 857 - 871
反应条件
tert-butylamine in benzene
8 h; Heating;
参考文献
Vovk, M. V.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 4 p. 654 - 658
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 4 p. 727 - 732
反应条件
in benzene
6 h; Heating;
参考文献
Vovk, M. V.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 4 p. 654 - 658
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 4 p. 727 - 732
反应条件
1: N2H4*H2O / bis-(2-hydroxy-ethyl) ether
2: (i) Br2, H2O, benzene, (ii) /BRN= 2323903/, Et3N
3: Se, nBu3N
4: benzene / Irradiation
View Scheme
参考文献
Back,T.G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 2079 - 2089
反应条件
1: 75 percent / NH2NH2*H2O / bis-(2-hydroxy-ethyl) ether / 18 h / Heating
2: 1) Br2, 2) Et3N / 1) benzene, 30 min, 0 deg C, 2) benzene, 5 h, rt
3: 0 Torr / bath temp.: 160 deg C
4: <Ag2CO3>infinite / 16.9 °C / 0.01 Torr
View Scheme
参考文献
Back,T.G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 2079 - 2089
