乙基2-甲基-5-苯基-3-糠酸酯合成路线 （共 16 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Takeda Pharmaceutical Company Limited
Patent: EP2210876 A1, 2010 ;
Location in patent: Page/Page column 70; 113 ;
反应条件
potassium acetate; silver carbonate in N,N-dimethyl-formamide T=80°C; 12 h; Inert atmosphere;
参考文献
He, Chuan; Guo, Sheng; Ke, Jie; Hao, Jing; Xu, Huan; Chen, Hongyi; Lei, Aiwen
Journal of the American Chemical Society, 2012 , vol. 134, # 13 p. 5766 - 5769
反应条件
Co(C20H8N4(C6H3(C(CH3)3)2)2(C6H3(NHCOCH(CH3)2)2)2) in 1,2-dichloro-benzene T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Cui, Xin; Xu, Xue; Wojtas, Lukasz; Kim, Martin M.; Zhang, X. Peter
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19981 - 19984
反应条件
silica gelsupported polyphosphoric acid T=80°C; 1 h;
参考文献
Aoyama, Tadashi; Nagaoka, Takashi; Takido, Toshio; Kodomari, Mitsuo
Synthesis, 2011 , # 4 art. no. F18910SS, p. 619 - 625
反应条件
aluminasuported sodium carbonate; silica gelsuported polyphosphoric acid in toluene T=80°C; 2 h;
参考文献
Aoyama, Tadashi; Nagaoka, Takashi; Takido, Toshio; Kodomari, Mitsuo
Synthesis, 2011 , # 4 art. no. F18910SS, p. 619 - 625
反应条件
aluminasuported sodium carbonate; silica gelsuported polyphosphoric acid in toluene T=110°C; 24 h;
参考文献
Aoyama, Tadashi; Nagaoka, Takashi; Takido, Toshio; Kodomari, Mitsuo
Synthesis, 2011 , # 4 art. no. F18910SS, p. 619 - 625
反应条件
aluminasuported sodium carbonate; silica gelsuported polyphosphoric acid in toluene T=80°C; 2 h;
参考文献
Aoyama, Tadashi; Nagaoka, Takashi; Takido, Toshio; Kodomari, Mitsuo
Synthesis, 2011 , # 4 art. no. F18910SS, p. 619 - 625
反应条件
[BMIm][HSO4] T=150°C; Paal-Knorr furan synthesis; 3 h; Sealed tubeNeat (no solvent);
参考文献
Wang, Gangqiang; Guan, Zhi; Tang, Rongchang; He, Yanhong
Synthetic Communications, 2010 , vol. 40, # 3 p. 370 - 377
反应条件
air; iron (III) perchlorate in acetic acid T=23°C;
参考文献
Yamada, Takashi; Iwahara, Yoko; Nishino, Hiroshi; Kurosawa, Kazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 5 p. 609 - 616
反应条件
potassium acetate; silver carbonate in N,N-dimethyl-formamide T=80°C; 12 h; Inert atmosphere;
参考文献
He, Chuan; Guo, Sheng; Ke, Jie; Hao, Jing; Xu, Huan; Chen, Hongyi; Lei, Aiwen
Journal of the American Chemical Society, 2012 , vol. 134, # 13 p. 5766 - 5769
