2-氯-4,6-二苯基嘧啶合成路线 （共 7 条）
反应条件
palladium diacetate; sodium carbonate; triphenylphosphine in ethylene glycol dimethyl ether T=70°C; Suzuki coupling; 24 h;
参考文献
Schomaker; Delia
Journal of Organic Chemistry, 2001 , vol. 66, # 21 p. 7125 - 7128
反应条件
trichlorophosphate 6 h; Heating / reflux;
参考文献
Ciba Specialty Chemicals Corporation
Patent: US6706215 B1, 2004 ;
Location in patent: Page column 40-41 ;
反应条件
sodium hydrogencarbonate; palladium diacetate in ethylene glycol dimethyl ether
参考文献
Parham, Amir Hossain; Pflumm, Christof; Mujica-Fernaud, Teresa; Buesing, Arne; Heil, Holger
Patent: US2012/97899 A1, 2012 ;
反应条件
1: 15 percent / toluene-p-sulphonic acid / acetic acid / 48 h / Heating 2: 47 percent / phosphoryl chloride View Scheme
参考文献
Nasielski; Standaert; Nasielski-Hinkens
Synthetic Communications, 1991 , vol. 21, # 7 p. 901 - 906
反应条件
hydroxylamine hydrochloride; triethylamine in ethanol 5 h;
参考文献
Moskalenko, G. G.; Sedova, V. F..; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 11 p. 1232 - 1236
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 11 p. 1523 - 1527
反应条件
hydroxylamine hydrochloride; triethylamine in ethanol 5 h;
参考文献
Moskalenko, G. G.; Sedova, V. F..; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 11 p. 1232 - 1236
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 11 p. 1523 - 1527
反应条件
sodium azide in dimethyl sulfoxide
T=90°C; 6 h;
参考文献
Krivopalov, V. P.; Nikolaenkova, E. B.; Sedova, V. F.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 977 - 981
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1222 - 1226
