(2-氧代环己基)氨基甲酸叔丁酯合成路线 (共 4 条)
反应条件
N-methyl-2-indolinone; tetrapropylammonium perruthennate in dichloromethane
参考文献
Sheppeck II, James E.; Gilmore, John L.; Yang, Anle; Chen, Xiao-Tao; Xue, Chu-Biao; Roderick, John; Liu, Rui-Qin; Covington, Maryanne B.; Decicco, Carl P.; Duan, James J.-W.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 5 p. 1413 - 1417
反应条件
1: methanol 2: TPAP; NMO / CH2Cl2 View Scheme
参考文献
Sheppeck II, James E.; Gilmore, John L.; Yang, Anle; Chen, Xiao-Tao; Xue, Chu-Biao; Roderick, John; Liu, Rui-Qin; Covington, Maryanne B.; Decicco, Carl P.; Duan, James J.-W.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 5 p. 1413 - 1417
反应条件
1: methanol 2: TPAP; NMO / CH2Cl2 View Scheme
参考文献
Sheppeck II, James E.; Gilmore, John L.; Yang, Anle; Chen, Xiao-Tao; Xue, Chu-Biao; Roderick, John; Liu, Rui-Qin; Covington, Maryanne B.; Decicco, Carl P.; Duan, James J.-W.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 5 p. 1413 - 1417
反应条件
1.1: trans-RuCl2[(R)-xylbinap][(S)-daipen]; KOH; H2 / propan-2-ol / 5 h / 25 °C / 6080.41 Torr
2.1: HCl / diethyl ether / 21 h / 25 °C
2.2: NaHCO3 / H2O; CH2Cl2 / 3 h / 25 °C
View Scheme
参考文献
Ohkuma, Takeshi; Ishii, Dai; Takeno, Hiroshi; Noyori, Ryoji
Journal of the American Chemical Society, 2000 , vol. 122, # 27 p. 6510 - 6511