2,2-二甲基-1,3-二氧环戊烷合成路线 （共 42 条）
反应条件
dimethyl-dichlorosilane T=20°C; 0.416667 h; also used catalyst (aq HCl), in ether, without Me2SiCl2;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Larionov, V. I.; Zlot-skii, S. S.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 6 p. 1394 - 1401,1229 - 1236
反应条件
indium trifluoromethanesulfonate T=20°C; 0.5 h; Neat (no solvent);
参考文献
Smith, Brendan M.; Graham, Andrew E.
Tetrahedron Letters, 2011 , vol. 52, # 47 p. 6281 - 6283
反应条件
K10; montmorillonite in toluene T=40 - 60°C; P=11251.1 Torr; 0.166667 h; Inert atmosphere; Product distribution / selectivity;
参考文献
SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.; BOS, Alouisius Nicolaas Renee; DERKS, Willem
Patent: WO2011/830 A1, 2011 ;
Location in patent: Page/Page column 10-12; 5/7; 7/7 ;
反应条件
copper(II) sulfate in acetone 24 h; Ambient temperature;
参考文献
Posner, Gary H.; Frye, Leah L.; Hulce, Martin
Tetrahedron, 1984 , vol. 40, # 8 p. 1401 - 1408
反应条件
phosphoric acid in ethylene glycol T=150°C;
参考文献
Sanderson, John R.; Lin, Jiang J.; Duranleau, Roger G.; Yeakey, Ernest L.; Marquis, Edward T.
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2859 - 2861
反应条件
tri-ruthenium(0)dodecacarbonyl T=100°C; 3 h;
参考文献
Zhou, Da-Yang; Yoneda, Eiji; Onitsuka, Kiyotaka; Takahashi, Shigetoshi
Chemical Communications, 2002 , # 23 p. 2868 - 2869
反应条件
amberlyst 15 T=60°C; 0.333333 h;
参考文献
Vol'Eva; Belostotskaya; Malkova; Komissarova; Kurkovskaya; Usachev; Makarov
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 5 p. 638 - 641
反应条件
copper(II) sulfate Ambient temperature;
参考文献
Posner, Gary H.; Frye, Leah L.; Hulce, Martin
Tetrahedron, 1984 , vol. 40, # 8 p. 1401 - 1408
反应条件
boron trifluoride diethyl etherate; mercury(II) oxide
参考文献
Croxall et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2805
反应条件
potassium hydroxide T=170°C;
参考文献
Schostakowskii; Gratschewa
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 355,358; engl. Ausg. S. 397, 400
