3-(三甲硅基)-1-丙醇合成路线 （共 32 条）
反应条件
hydrogenchloride Heating;
参考文献
Smirnova,G.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, # 12 p. 2684 - 2688,2718 - 2721
反应条件
in diethyl ether Heating;
参考文献
Mironov,V.F.; Pogonkina,N.A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1960 , p. 1856 - 1859
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 1998 - 2002
反应条件
oxidation; Yield given;
参考文献
Soderquist, John A.; Brown, Herbert C.
Journal of Organic Chemistry, 1980 , vol. 45, # 18 p. 3571 - 3578
反应条件
(i) Na, toluene, (ii) KOH, EtOH; Multistep reaction;
参考文献
Andreev,D.N.; Afanas'eva,G.S.
J. Gen. Chem. USSR (Engl. Transl.), 1966 , vol. 36, p. 1628 - 1633,1629 - 1632
反应条件
phosphorus tribromide in not given
参考文献
Sommer; Van Strien; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 3056
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Gmelin Handbook: Si: MVol.C, 9, page 28 - 32
Full Text Show Details
Dow Corning Corp.
Patent: US2557802 , 1951 ;
C. A., 1952 , p. 1026
参考文献
Merrell Dow Pharmaceuticals, Inc.
Patent: US5252587 A1, 1993 ;
反应条件
1: 81 percent / PBr3 / diethyl ether / 0 °C 2: 1.) Li / 1.) diethylether, RT, 1 h, 2.) diethylether, RT, 2h 3: 68 percent / PBr3 / diethyl ether / 0 °C View Scheme
参考文献
Maercker, Adalbert; Eckers, Mechthild; Passlack, Michael
Journal of Organometallic Chemistry, 1980 , vol. 186, # 2 p. 193 - 205
反应条件
1: 100 percent / triethylamine / diethyl ether / 18 h / 25 °C 2: 99 percent / NaI / acetone / 18 h / Heating View Scheme
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
trifluoroacetic acid in benzene
参考文献
Mironov,V.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, p. 813 - 816,776 - 778
反应条件
2: aq. NH3 View Scheme
参考文献
Mironov,V.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1966 , vol. 36, # 10 p. 1860,1852
