3-(三甲硅基)-1-丙醇合成路线 （共 32 条）
反应条件
(i) Py, (ii) liq. NH3; Multistep reaction;
参考文献
Fessenden; Coon
Journal of medicinal chemistry, 1965 , vol. 8, # 5 p. 604 - 608
参考文献
Kvicalova, Magdalena; Cermak, Jan; Blechta, Vratislav; Schraml, Jan
Collection of Czechoslovak Chemical Communications, 1997 , vol. 62, # 5 p. 816 - 820
反应条件
1: triphenyl phosphine, diethyl azodicarboxylate 2: hydrazine View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, # 7 p. 2219 - 2220
反应条件
pyridinium chlorochromate
参考文献
Shiner, V. J.; Ensinger, Mark W.; Rutkowske, Randy D.
Journal of the American Chemical Society, 1987 , vol. 109, # 3 p. 804 - 809
反应条件
1: pyridine
2: LiBr / 1,2-dimethoxy-ethane / Heating
3: LDA-HMPA / tetrahydrofuran
View Scheme
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
1: pyridine
2: LiBr / 1,2-dimethoxy-ethane / Heating
3: LDA-HMPA / tetrahydrofuran
View Scheme
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
1: pyridine
2: NaI / acetone
3: LDA-HMPA / tetrahydrofuran
4: LiI, collidine / dimethylformamide / 140 °C
View Scheme
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
1: pyridine
2: NaI / acetone
3: LDA-HMPA / tetrahydrofuran
View Scheme
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
(2-chloro-1,2,2-trifluoro-ethyl)-diethyl-amine in diethyl ether
参考文献
Puchnarevic,V.B. et al.
Collection of Czechoslovak Chemical Communications, 1974 , vol. 39, p. 2616 - 2620
