3,7-二甲基-6-辛烯-1-炔基-3-醇合成路线 （共 58 条）
反应条件
1: 95 percent / phenol / 48 h / 140 °C
2: 92 percent / aq.KOH / tetrahydrofuran / 2 h / 90 °C
View Scheme
参考文献
Lee, Eun; Lee, Dae Sung; Choi, Yoon Whan; Lee, Kwang Ho
Tetrahedron Letters, 1992 , vol. 33, # 44 p. 6673 - 6676
反应条件
palladium diacetate; 4-ethyl-2,6,7-trioxa-1-phosphabicyclo-[2,2,2]-octane in chloroform
T=60°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Trost, Barry M.; Lautens; Chan; Jebaratnam; Mueller
Journal of the American Chemical Society, 1991 , vol. 113, # 2 p. 636 - 644
反应条件
allylindium sesquiiodide in N,N-dimethyl-formamide
Heating;
参考文献
Araki, Shuki; Imai, Akira; Shimizu, Ken; Yamada, Masafumi; Mori, Akihiro; Butsugan, Yasuo
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1841 - 1847
反应条件
indium
1.) DMF, 2.) 110 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Araki, Shuki; Imai, Akira; Shimizu, Ken; Yamada, Masafumi; Mori, Akihiro; Butsugan, Yasuo
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1841 - 1847
反应条件
indium
1.) DMF, 2.) heating; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Araki, Shuki; Imai, Akira; Shimizu, Ken; Yamada, Masafumi; Mori, Akihiro; Butsugan, Yasuo
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1841 - 1847
参考文献
Firmenich
Patent: FR2259091US4147672 , 19751979 ;
Chem.Abstr., 1979 , vol. 91, # 19986
反应条件
1: With potassium hydroxide; ammonia in water
T=25°C; 22 h; Autoclave;
2: With sulfuric acid in water
参考文献
DSM IP Assets B.V.
Patent: EP1808426 A1, 2007 ;
Location in patent: Page/Page column 3-4 ;
反应条件
N-bromosuccinmide in tetrachloromethane
T=20°C;
参考文献
Baskaran, Sundarababu; Islam, Imadul; Chandrasekaran, Srinivasan
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 891 - 895
