2,9-二氯-1,10-菲罗啉合成路线 （共 23 条）
参考文献
Lewis, Jack; O'Donoghue, Timothy D.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 736 - 742
反应条件
thiourea in ethanol 3 h; Reflux;
参考文献
Krapcho, A. Paul; Sparapani, Silvia; Leenstra, Amber; Seitz, Joshua D.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3195 - 3197
反应条件
tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; sodium carbonate in water; toluene T=100°C; Suzuki-Miyaura Coupling; 5 h; Inert atmosphere;
参考文献
Kuritani, Masumi; Tashiro, Shohei; Shionoya, Mitsuhiko
Chemistry - An Asian Journal, 2013 , vol. 8, # 7 p. 1368 - 1371
反应条件
in methanol; toluene 72 h; Heating;
参考文献
Pijper; Van der Goot; Timmerman; Nauta Th.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 5 p. 399 - 404
反应条件
sodium methylate 19 h; Heating;
参考文献
Krapcho, A. Paul; Sparapani, Silvia
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 4 p. 1167 - 1170
反应条件
barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether Suzuki reaction; 16 h; Heating;
参考文献
Luening, Ulrich; Abbass, Michael; Fahrenkrug, Frank
European Journal of Organic Chemistry, 2002 , # 19 p. 3294 - 3303
反应条件
hydrazine hydrate
Heating;
参考文献
Lewis, Jack; O'Donoghue, Timothy D.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 736 - 742
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Stille coupling; 40 h; Heating;
参考文献
Zong, Ruifa; Thummel, Randolph P.
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 10800 - 10801
反应条件
bis(triphenylphosphine)palladium(II)-chloride in N,N-dimethyl-formamide
T=80°C; 60 h;
参考文献
Zong, Ruifa; Wang, Dong; Hammitt, Richard; Thummel, Randolph P.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 167 - 175
反应条件
in N,N-dimethyl-formamide
T=20°C; 20 h;
参考文献
Krapcho, A. Paul; Sparapani, Silvia; Leenstra, Amber; Seitz, Joshua D.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3195 - 3197
