2-溴-N-(4-甲氧基苯)乙酰胺合成路线 (共 5 条)
反应条件
triethylamine in chloroform T=-50 - -15°C;
参考文献
Vloon; Kruk; Pandit; Hofs; McVie
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 20 - 24
反应条件
in acetonitrile T=0 - 20°C; 1 h;
参考文献
Samanta, Sanjay; Lim, Ting Liang; Lam, Yulin
ChemMedChem, 2013 , vol. 8, # 6 p. 994 - 1001
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=-5 - 20°C;
参考文献
Chen, Xiaofang; Wang, Li; Du, Yu; Wu, Yanbin; Jia, Xiaojian; Yang, Yuan; Hong, Bin
Molecules, 2011 , vol. 16, # 11 p. 9178 - 9193
反应条件
N(Et)4ClO4; bromomalonic acid diethyl ester in N,N-dimethyl-formamide
electroreduction, Hg cathode;
参考文献
Casadei, Maria Antonietta; Rienzo, Barbara Di; Inesi, Achille; Moracci, Franco Micheletti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 379 - 382
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
electroreduction, Hg cathode;
参考文献
Casadei, Maria Antonietta; Rienzo, Barbara Di; Inesi, Achille; Moracci, Franco Micheletti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 379 - 382