反应条件
sodium hydride 1.) THF, RT, 15 min, 2.) THF, reflux, 20 h; Yield given. Multistep reaction;
参考文献
MERCK SHARP and DOHME CORP.; SEGANISH, W. Michael; BRUMFIELD, Stephanie Nicole; LIM, Jongwon; MATASI, Julius, J.; MCELROY, William, T.; TULSHIAN, Dean, B.; LAVEY, Brian, J.; ALTMAN, Michael, D.; GIBEAU, Craig, R.; LAMPE, John William; METHOT, Joey; ZHU, Liang
Patent: WO2013/66729 A1, 2013 ;
Location in patent: Page/Page column 148; 149 ;
WO 2013/066729 A1