2,4-二氯-N-羟基苯甲酰氯合成路线 （共 7 条）
反应条件
N-(tert-butyl)-N-chloro-cyanamide in dichloromethane T=20°C;
参考文献
Kumar, Vinod; Kaushik
Tetrahedron Letters, 2006 , vol. 47, # 9 p. 1457 - 1460
反应条件
1: aq. NH2OH*HCl; AcONa / ethanol / 12 h 2: N-chlorosuccinimide; pyridine / CHCl3; tetrahydrofuran / 2 h View Scheme
参考文献
Gucma, Miroslaw; Golebiewski, W. Marek
Monatshefte fur Chemie, 2010 , vol. 141, # 4 p. 461 - 469
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Das, Sushanta K.; Balasubrahmanyam, S. N.
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4232 - 4236
反应条件
triethylamine in chloroform
参考文献
Trepanier; Faith; Eble
Journal of medicinal chemistry, 1970 , vol. 13, # 4 p. 729 - 733
反应条件
1: 97 percent / aq. NaN3 / methanol 2: acetonitrile / 12 h / 20 °C View Scheme
参考文献
Johnson, Wynona M.; Littler, Stuart W.; Skene, Colin E.
Australian Journal of Chemistry, 1993 , vol. 46, # 3 p. 315 - 324
反应条件
1.1: NaOMe / methanol 1.2: methanol / 4 h / 0 °C 2.1: 100 percent / LiAlH4 / diethyl ether / 1 h / 40 °C View Scheme
参考文献
Roy, Amrendra K.; Batra, Sanjay
Synthesis, 2003 , # 9 p. 1347 - 1356
反应条件
1: acetoacetic acid methyl ester With sodium methylate in methanol
2: 2,4-dichloro-N-hydroxybenzenecarboximidoyl chloride in methanol
T=0°C; 4 h;
参考文献
Roy, Amrendra K.; Batra, Sanjay
Synthesis, 2003 , # 9 p. 1347 - 1356
