二[(九氟丁基)磺酰基]甲烷合成路线 （共 3 条）
反应条件
(trimethyl)silylmethyllithium in pentane T=2 - 20°C; 61 h;
参考文献
The Institute of Applied Catalysis
Patent: US6664380 B1, 2003 ;
Location in patent: Page column 15-16 ;
参考文献
Barrett, Anthony G.M.; Bouloc, Nathalie; Christopher Braddock; Catterick, David; Chadwick, David; White, Andrew J.P.; Williams, David J.
Tetrahedron, 2002 , vol. 58, # 20 p. 3835 - 3840
反应条件
in diethyl ether 1 h at 30-40°C, then 1.5 h at 35°C, 0.5 h at 50°C; acidification of the mixt. with 3 N HCl, distn. of the organic phase;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
