3-乙酰基庚烷-2,6-二酮合成路线 （共 8 条）
反应条件
cerium(III) chloride; sodium iodide in neat (no solvent) 6 h; Ambient temperature;
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Bellucci, Maria Cristina; Marcantoni, Enrico; Sambri, Letizia; Torregiani, Elisabetta
European Journal of Organic Chemistry, 1999 , # 3 p. 617 - 620
反应条件
oxygen in tetrahydrofuran T=30°C; aerobic oxidation-Michael addition; P=760.051 Torr; 20 h;
参考文献
Yoo, Woo-Jin; Miyamura, Hiroyuki; Kobayashi, Shu
Journal of the American Chemical Society, 2011 , vol. 133, # 9 p. 3095 - 3103
反应条件
2-(tert-butylimino)-2-(diethylamino)-1,3-dimethylperhydro-1,3,2-diazaphosphorine polymer bound in tetrahydrofuran T=20°C; 4 h; Inert atmosphere;
参考文献
Allais, Christophe; Lieby-Muller, Frederic; Rodriguez, Jean; Constantieux, Thierry
European Journal of Organic Chemistry, 2013 , # 19 p. 4131 - 4145
反应条件
N-ethyl-N,N-diisopropylamine in ethanol Michael addition;
参考文献
Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.; Pombo-Villar, Esteban
Tetrahedron, 2005 , vol. 61, # 45 p. 10757 - 10773
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in water T=70°C; 48 h;
参考文献
Bassetti, Mauro; Cerichelli, Giorgio; Floris, Barbara
Gazzetta Chimica Italiana, 1991 , vol. 121, # 12 p. 527 - 532
反应条件
ammonium acetate in toluene 24 h; Molecular sieveReflux;
参考文献
Lieby-Muller, Frederic; Allais, Christophe; Constantieux, Thierry; Rodriguez, Jean
Chemical Communications, 2008 , # 35 p. 4207 - 4209
反应条件
triethylamine; Methanesulfonyl azide in acetonitrile
T=23°C; 1.5 h;
参考文献
Jung, Michael E.; Min, Sun-Joon; Houk; Ess, Daniel
Journal of Organic Chemistry, 2004 , vol. 69, # 26 p. 9085 - 9089
反应条件
H-ZSM-5 zeolite in benzene
T=199.9°C; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Reddy, P. Veera; Prakash, Adekkanattu M.; Chakrabarty, Dipak K.; Bhat, Sujata V.
Journal of Chemical Research, Synopses, 1997 , # 8 p. 306 - 307
