反应条件
1: 30 percent / HMPT / Ambient temperature
2: 37 percent / NaI / acetone / Heating
3: 1.) EtMgBr, Mg / 1.) THF, reflux, 3 h, 2.) THF, RT, overnight
5: LiAlH4 / tetrahydrofuran / 4.5 h / Ambient temperature
View Scheme
参考文献
Bricard; Kunesch
Synthetic Communications, 1993 , vol. 23, # 18 p. 2547 - 2558
