反应条件
oleic acid in further solvent(s) Eu(CF3COO)3 (0.5 mmol) and KCF3COO (0.5 mmol) added to oleic acid; placed under N2; heated to 100°C over 2 h (vac. applied periodically);represurized with N2; heated (280°C, 40 min); cooled to room temp.; EtOH added; ppt. collected by filtration; washed with EtOH; dissolved in toluene; dropped onto carbon coated grid; dried;
参考文献
Rahman, Paula; Green, Mark; Heatherington, Crispin; Karlsson, Lisa; Kallumadil, Mathew
Chemical Communications, 2010 , vol. 46, # 9 p. 1517 - 1519
