in dichloromethane to soln. of ClSnBu3 in CH2Cl2 is added AgSO3CF3, mixt. is stirred at room temp. for 1 h; filtration, CH2Cl2 is removed under reduced pressure and inert atmosphere, residue is heated to 65°C and 0.01 mmHg;
参考文献
Farah, Dan; Swami, Kamal; Kuivila, Henry G.
Journal of Organometallic Chemistry, 1992 , vol. 429, # 3 p. 311 - 334
Shackelford, S. A.; Chapman, R. D.; Andreshak, J. L.; Herrlinger, S. P.; Hildreth, R. A.; Smith, J. C.
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 123
