反应条件
1: tert-butyl acetyl(benzyl)carbamate With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78°C; 2: With methanol in tetrahydrofuran; hexane 0.5 h; 3: acrylic acid methyl ester With samarium diiodide; boron trifluoride diethyl etherate in tetrahydrofuran; hexane; tert-butyl alcohol T=-40°C; Michael addition;
参考文献
Liu, Xue-Kui; Zheng, Xiao; Ruan, Yuan-Ping; Ma, Jie; Huang, Pei-Qiang
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 6 p. 1275 - 1284