1-碘-2-甲基-3,5-二硝基苯合成路线 （共 3 条）
反应条件
reagent "I(1+)" in sulfuric acid T=100°C; Iodination; 6.5 h;
参考文献
Chaikovskii, V. K.; Kharlova, T. S.; Filimonov, V. D.
Russian Chemical Bulletin, 1999 , vol. 48, # 7 p. 1291 - 1294
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1999 , # 7 p. 1303 - 1306
反应条件
sulfuric acid; nitric acid
参考文献
Kapil,R.S.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1036 - 1037
反应条件
1: H2S, aq. NH3 / dioxane
2: (i) NaNO2, H3PO4, H2SO4, (ii) KI
3: Sn, aq. HCl
4: (i) NaNO2, H3PO4, H2SO4, (ii) KI
View Scheme
参考文献
Arotsky,J. et al.
Journal of the Chemical Society [Section] C: Organic, 1970 , p. 1480 - 1485
