4-氟-7-硝基苯并-2-氧杂-1,3-二唑合成路线 （共 4 条）
反应条件
sodium nitrate; sulfuric acid in water T=0°C; 0.0666667 h; Inert atmosphere;
参考文献
Jung, Michael E.; Dong, Timothy A.; Cai, Xiaolu
Tetrahedron Letters, 2011 , vol. 52, # 20 p. 2533 - 2535
反应条件
1: sodium azide / dimethyl sulfoxide / 2.5 h / 23 °C / Inert atmosphere 2: sodium nitrate; sulfuric acid / water / 0.07 h / 0 °C / Inert atmosphere View Scheme
参考文献
Jung, Michael E.; Dong, Timothy A.; Cai, Xiaolu
Tetrahedron Letters, 2011 , vol. 52, # 20 p. 2533 - 2535
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 23 °C / Inert atmosphere 2: sodium azide / dimethyl sulfoxide / 2.5 h / 23 °C / Inert atmosphere 3: sodium nitrate; sulfuric acid / water / 0.07 h / 0 °C / Inert atmosphere View Scheme
参考文献
Jung, Michael E.; Dong, Timothy A.; Cai, Xiaolu
Tetrahedron Letters, 2011 , vol. 52, # 20 p. 2533 - 2535
反应条件
sodium hydrogencarbonate in water; acetonitrile T=23°C; 28 h; DarknessInert atmosphere;
参考文献
Jung, Michael E.; Dong, Timothy A.; Cai, Xiaolu
Tetrahedron Letters, 2011 , vol. 52, # 20 p. 2533 - 2535
