4-[2-羟基-3-[(1-甲基乙基)氨基]丙氧基]苯乙腈合成路线 (共 6 条)
反应条件
in methanol T=20°C; P=760.051 Torr; 20 h;
参考文献
Akisanya, Joseph; Parkins, Adrian W.; Steed, Jonathan W.
Organic Process Research and Development, 1998 , vol. 2, # 4 p. 274 - 276
反应条件
1: N,N-dimethyl-formamide 2: piperidine / 6 h / 95 - 100 °C 3: methanol / 20 h / 20 °C / 760.05 Torr View Scheme
参考文献
Akisanya, Joseph; Parkins, Adrian W.; Steed, Jonathan W.
Organic Process Research and Development, 1998 , vol. 2, # 4 p. 274 - 276
反应条件
1: piperidine / 6 h / 95 - 100 °C 2: methanol / 20 h / 20 °C / 760.05 Torr View Scheme
参考文献
Akisanya, Joseph; Parkins, Adrian W.; Steed, Jonathan W.
Organic Process Research and Development, 1998 , vol. 2, # 4 p. 274 - 276
参考文献
Eckardt; Carstens; Fiedler
Pharmazie, 1975 , vol. 30, # 10 p. 633 - 637
反应条件
bis(dimethylphosphinous acid-kP)dimethylphosphinyl-kP-hydridoplatinum(II) in ethanol; water 72 h; Reflux;
参考文献
Akisanya, Joseph; Parkins, Adrian W.; Steed, Jonathan W.
Organic Process Research and Development, 1998 , vol. 2, # 4 p. 274 - 276
参考文献
ICI
Patent: DE2007751 , 1970 ;
Chem.Abstr., 1970 , vol. 73, # 120318