2,3-二苯基噻唑烷-4-酮合成路线 （共 12 条）
反应条件
T=250°C; 10 h; MechanismProduct distribution;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 57, # 34 p. 255 - 260
反应条件
T=250°C; 10 h; MechanismProduct distribution;
参考文献
Atalla, A. A.; Gaber, A. M.; El-Dean, A. M. Kamal; Mohamed, Th. A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 57, # 34 p. 255 - 260
反应条件
1: benzyl alcohol With 1-propanephosphonic acid cyclic anhydride in dimethyl sulfoxide; ethyl acetate
T=0 - 25°C; Inert atmosphere;
2: mercaptoacetic acid; aniline in dimethyl sulfoxide; ethyl acetate
T=25°C; Inert atmosphere;
参考文献
Sharath Kumar, Kothanahally S.; Swaroop, Toreshettahally R.; Harsha, Kachigere B.; Narasimhamurthy, Kereyagalahally H.; Rangappa, Kanchugarakoppal S.
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5619 - 5623
反应条件
HClO4 immobilized on silica in toluene
T=100°C; 4 h; Green chemistry; Catalytic behavior; Reagent/catalystSolventTemperatureTime;
参考文献
Kumar, Dinesh; Sonawane, Mukesh; Pujala, Brahmam; Jain, Varun K.; Bhagat, Srikant; Chakraborti, Asit K.
Green Chemistry, 2013 , vol. 15, # 10 p. 2872 - 2884
反应条件
piperidine in ethanol
2 h; Heating;
参考文献
Elbannany; Azim Hady Ibrahim
Pharmazie, 1986 , vol. 41, # 2 p. 144 - 145
反应条件
in ethanol
48 h; Heating;
参考文献
Tierney, John; Sheridan, Douglas; Mascavage, Linda; Gorbecheva, Daniela; Ripp, Michelle; Son, Sonjoo
Heterocyclic Communications, 2005 , vol. 11, # 3-4 p. 215 - 222
反应条件
in benzene-d6
T=30°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Bolognese, Adele; Correale, Gaetano; Manfra, Michele; Lavecchia, Antonio; Novellino, Ettore; Barone, Vincenzo
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 19 p. 2809 - 2813
反应条件
1: benzene / Heating
2: benzene / 0.17 h / 30 °C / microwave irradiation
View Scheme
参考文献
Bolognese, Adele; Correale, Gaetano; Manfra, Michele; Lavecchia, Antonio; Novellino, Ettore; Barone, Vincenzo
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 19 p. 2809 - 2813
反应条件
1: benzene / Heating
2: benzene / 0.17 h / 30 °C / microwave irradiation
View Scheme
参考文献
Bolognese, Adele; Correale, Gaetano; Manfra, Michele; Lavecchia, Antonio; Novellino, Ettore; Barone, Vincenzo
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 19 p. 2809 - 2813
反应条件
in diethyl ether
Heating;
参考文献
Satsumabayashi,S. et al.
Synthesis, 1977 , p. 881 - 883
