in tetrachloromethane byproducts: S8; reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products;; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
in methanol; water; benzene SnCl2*2H2O in MeOH-water added rapidly with vigorous stirring to SnCl4(S4N4)2 in refluxing dry benzene, soln. left for 30 min; mixt. filtered at 0°C, crude solid recrystd. from CH3NO2;
参考文献
Banister, Arthur J.; Fielder, Andrew J.; Hey, Richard G.; Smith, Nigel R. M.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , # 8 p. 1457 - 1460
in water; acetone
byproducts: nitrite; aq. acetone; formation of NO3(1-) containing compound;;
参考文献
Goehring, M.; Weiss, J.; Zirker, G.
Z. Anorg. Chem., 1955 , vol. 278, p. 1 - 11
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Gmelin Handbook: S: MVol.B3, 15, page 1560 - 1562
