1: With chloro-trimethyl-silane; 1,2-ferrocenediyl(-PPh2=C(COPh)-N=C(Me)-) in dichloromethane
T=20°C; 3 h;
2: With hydrogenchloride in diethyl ether
T=20°C; 1 h; Title compound not separated from byproducts;
参考文献
Paek, Seung Hwan; Shim, Sang Chul; Cho, Chan Sik; Kim, Tae-Jeong
Synlett, 2003 , # 6 p. 849 - 851
1: 90 percent / 72percent HClO4 / H2O / 80 °C
2: 36 percent / NaH / tetrahydrofuran / 24 h / Heating
View Scheme
参考文献
Nakatsuji, Yohji; Nakamura, Tetsuya; Okahara, Mitsuo; Dishong, Dennis M.; Gokel, George W.
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1237 - 1242
