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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苄基缩水甘油醚
合成路线
（共 145 条）
2930-05-4
苄基缩水甘油醚
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
173917-47-0
反应条件
iso-propylmagnesium bromide in various solvent(s) 2 h; -15 deg C - room temperature;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
2930-05-4
苄基缩水甘油醚
+
14618-80-5
(R)-苄氧甲基环氧乙烷
反应条件
Bacillus megaterium ECU1001 epoxide hydrolase in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 2 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
109-65-9
正溴丁烷
+
2930-05-4
苄基缩水甘油醚
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
137226-14-3
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
+
108-86-1
溴代苯
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
173917-50-5
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
+
53963-10-3
2-(6-溴己氧基)四氢-2H-吡喃
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C - room temperature, 120 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
+
507-20-0
氯代叔丁烷
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
173917-48-1
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
+
112-29-8
癸基溴
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
173917-46-9
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
+
100-44-7
苄基氯
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
92527-69-0
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
+
75-26-3
2-溴丙烷
→
反应条件
13071-59-5
(R)-(+)-1-苄基丙三醇
+
173917-47-0
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C - room temperature, 120 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Poppe; Recseg; Novak
Synthetic Communications, 1995 , vol. 25, # 24 p. 3993 - 4000
2930-05-4
苄基缩水甘油醚
+
124-38-9
二氧化碳
→
反应条件
949-97-3
反应条件
potassium carbonate; zinc dibromide; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in dimethyl sulfoxide T=80°C; 24 h; Inert atmosphere;
参考文献
Liu, Xiang; Cao, Changsheng; Li, Yunfei; Guan, Pei; Yang, Longguang; Shi, Yanhui
Synlett, 2012 , vol. 23, # 9 p. 1343 - 1348
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