1: chelidamic acid With N-(chloromethylene)-N-methylmethanaminium chloride; triethylamine; N,N-dimethyl-formamide in acetonitrile T=75°C; P=5171.62 Torr; 2: methanol in acetonitrile
参考文献
Battilocchio, Claudio; Baumann, Marcus; Baxendale, Ian R.; Biava, Mariangela; Kitching, Matthew O.; Ley, Steven V.; Martin, Rainer E.; Ohnmacht, Stephan A.; Tappin, Nicholas D. C.
Synthesis, 2012 , vol. 44, # 4 p. 635 - 647
sulfuric acid in water T=20°C; Esterification; 12 h;
参考文献
Iglesias, Carlos Platas; Elhabiri, Mourad; Hollenstein, Marcel; Buenzli, Jean-Claude G.; Piguet, Claude
Journal of the Chemical Society, Dalton Transactions, 2000 , # 13 p. 2031 - 2043
1: 1 h 2: 98 percent / aq. NaOH / 1 h / Heating 3: 61 percent / conc. H2SO4 / H2O / 12 h / 20 °C View Scheme
参考文献
Iglesias, Carlos Platas; Elhabiri, Mourad; Hollenstein, Marcel; Buenzli, Jean-Claude G.; Piguet, Claude
Journal of the Chemical Society, Dalton Transactions, 2000 , # 13 p. 2031 - 2043
1: phenylphosphonic dichloride / 2 h / 120 °C 2: 1 h 3: 98 percent / aq. NaOH / 1 h / Heating 4: 61 percent / conc. H2SO4 / H2O / 12 h / 20 °C View Scheme
参考文献
Iglesias, Carlos Platas; Elhabiri, Mourad; Hollenstein, Marcel; Buenzli, Jean-Claude G.; Piguet, Claude
Journal of the Chemical Society, Dalton Transactions, 2000 , # 13 p. 2031 - 2043
1: ammonium hydroxide / 4.5 h / 45 °C / 3878.71 Torr / Sonication 2: N-(chloromethylene)-N-methylmethanaminium chloride; triethylamine; N,N-dimethyl-formamide / acetonitrile / 75 °C / 5171.62 Torr View Scheme
参考文献
Battilocchio, Claudio; Baumann, Marcus; Baxendale, Ian R.; Biava, Mariangela; Kitching, Matthew O.; Ley, Steven V.; Martin, Rainer E.; Ohnmacht, Stephan A.; Tappin, Nicholas D. C.
Synthesis, 2012 , vol. 44, # 4 p. 635 - 647
