反应条件
1: pyridine / tetrahydrofuran / 0.33 h / 20 °C
2: 1,8-diazabicyclo[5.4.0]-7-undecene / tetrahydrofuran; H2O / 1 h / Heating
3: NaHCO3 / tetrahydrofuran; H2O / 0 °C
4: aq. HCl / acetic acid / 2 h / 70 °C
5: NaClO2; NaH2PO4; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O / 3 h / 0 - 20 °C
View Scheme
参考文献
Ohmoto; Yamamoto; Horiuchi; Kojima; Hachiya; Hashimoto; Kawamura; Nakai; Toda
Synlett, 2001 , # 2 p. 299 - 301
