1-硫代-b-D-吡喃葡萄糖苷对甲苯酯合成路线 (共 42 条)
反应条件
sodium methylate T=0°C; 0.166667 h;
参考文献
Peri, Francesco; Cipolla, Laura; Forni, Eleonora; Nicotra, Francesco
Monatshefte fur Chemie, 2002 , vol. 133, # 4 p. 369 - 382
反应条件
1: 79 percent / SnCl4 / CH2Cl2 2: 100 percent / NaOMe / methanol View Scheme
参考文献
Tran, Anh-Tuan; Burden, Richard; Racys, Daugirdas T.; Carmen Galan
Chemical Communications, 2011 , vol. 47, # 15 p. 4526 - 4528
反应条件
1: 78 percent / tin(IV) chloride / CH2Cl2 / 24 h / 20 °C 2: 99 percent / K2CO3 / tetrahydrofuran; methanol / 5 h / 20 °C View Scheme
参考文献
Motawia; Olsen; Enevoldsen; Marcussen; Moller
Carbohydrate Research, 1995 , vol. 277, # 1 p. 109 - 123
反应条件
tetra-(n-butyl)ammonium iodide; zinc(II) iodide in 1,2-dichloro-ethane T=60°C; 8 h; Yields of byproduct given;
参考文献
Hanessian, Stephen; Guindon, Yvan
Carbohydrate Research, 1980 , vol. 86, p. C3 - C6
反应条件
1: 78 percent / tin(IV) chloride / CH2Cl2 / 24 h / 20 °C 2: 99 percent / K2CO3 / tetrahydrofuran; methanol / 5 h / 20 °C View Scheme
参考文献
Nicolaou; Winssinger; Pastor; DeRoose
Journal of the American Chemical Society, 1997 , vol. 119, # 2 p. 449 - 450
反应条件
OleD A242V/S132F/P67T triple mutant; tris(hydroxymethyl)methylamine hydrochloride; magnesium chloride T=25°C; pH=8.0; 16 h; Enzymatic reaction; stereoselective reaction;
参考文献
Gantt, Richard W.; Goff, Randal D.; Williams, Gavin J.; Thorson, Jon S.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 46 p. 8889 - 8892
反应条件
1: zinc(II) iodide / dichloromethane / 2 h / 20 °C / Inert atmosphere 2: water; triethylamine / methanol / 20 °C / Inert atmosphere View Scheme
参考文献
Balmond, Edward I.; Coe, Diane M.; Galan, M. Carmen; McGarrigle, Eoghan M.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 36 p. 9152 - 9155
反应条件
1: 87 percent / tetrabutylammonium hydrogen sulfate; Na2CO3 / CH2Cl2 / 0.75 h / 25 °C 2: 99 percent / Na / methanol / 3 h / 20 °C View Scheme
参考文献
Larsen, Kim; Olsen, Carl Erik; Motawia, Mohammed Saddik
Carbohydrate Research, 2003 , vol. 338, # 2 p. 199 - 202
反应条件
2-chloro-1,3-dimethylimidazolinium chloride
参考文献
Upadhyay, Sunil K.; Jursic, Branko S.
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1835 - 1838
反应条件
sodium methylate; tin(IV) chloride 1.) PhH, 60 deg C; 2.) MeOH, 25 deg C; Yield given. Multistep reaction;
参考文献
Nicolaou, K. C.; Randall, J. L.; Furst, G. T.
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5556 - 5558