2-乙基-3-羟基-1,4-萘二酮合成路线 （共 20 条）
参考文献
Farina, F.; Fernandez, E.; Gimeno, V.; Valderrama, J. A.
Anales de Quimica, 1995 , vol. 91, # 3-4 p. 220 - 229
反应条件
selenium(IV) oxide; ethanol
参考文献
Fieser; Brown
Journal of the American Chemical Society, 1949 , vol. 71, p. 3615
反应条件
1: 90 percent / 30percent H2O2, aq. 30percent Na2CO3 / ethanol / 45 °C
2: 80 percent / 50percent aq. H2SO4 / 5 h
View Scheme
参考文献
Farina, F.; Fernandez, E.; Gimeno, V.; Valderrama, J. A.
Anales de Quimica, 1995 , vol. 91, # 3-4 p. 220 - 229
反应条件
in tert-butyl alcohol
Heating;
参考文献
Yakubovskaya; Kochergina; Denisenko; Berdyshev; Glazunov; Anufriev
Russian Chemical Bulletin, 2006 , vol. 55, # 2 p. 301 - 305
反应条件
1: 90 percent / benzene / 8 h / 110 °C
2: 84 percent / AcOH, Na2Cr2O7*2H2O, aq. H2SO4 / a) 80-90 deg C, 1 h, b) RT, 12 h
3: 90 percent / 30percent H2O2, aq. 30percent Na2CO3 / ethanol / 45 °C
4: 80 percent / 50percent aq. H2SO4 / 5 h
View Scheme
参考文献
Farina, F.; Fernandez, E.; Gimeno, V.; Valderrama, J. A.
Anales de Quimica, 1995 , vol. 91, # 3-4 p. 220 - 229
反应条件
1: 84 percent / AcOH, Na2Cr2O7*2H2O, aq. H2SO4 / a) 80-90 deg C, 1 h, b) RT, 12 h
2: 90 percent / 30percent H2O2, aq. 30percent Na2CO3 / ethanol / 45 °C
3: 80 percent / 50percent aq. H2SO4 / 5 h
View Scheme
参考文献
Farina, F.; Fernandez, E.; Gimeno, V.; Valderrama, J. A.
Anales de Quimica, 1995 , vol. 91, # 3-4 p. 220 - 229
反应条件
potassium hydroxide in methanol
1 h; Reflux;
参考文献
Nasiri, Hamid Reza; Madej, M. Gregor; Panisch, Robin; Lafontaine, Michael; Bats, Jan W.; Lancaster, C. Roy D.; Schwalbe, Harald
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9530 - 9541
反应条件
1: (NH4)2S2O8; silver nitrate / acetonitrile; water / 80 °C
2: potassium hydroxide / methanol / 1 h / |Reflux
View Scheme
参考文献
Nasiri, Hamid Reza; Madej, M. Gregor; Panisch, Robin; Lafontaine, Michael; Bats, Jan W.; Lancaster, C. Roy D.; Schwalbe, Harald
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9530 - 9541
反应条件
potassium hydroxide; air
参考文献
Soliman; Latif
Journal of the Chemical Society, 1944 , p. 55
反应条件
sodium hydroxide; air
参考文献
Jain; Seshadri
Journal of Scientific and Industrial Research, 1954 , vol. 13 B, p. 756
