1,4,7,10-四氮杂环十二烷合成路线 （共 64 条）
反应条件
in chloroform T=20°C;
参考文献
Tetrahedron Letters, , vol. 47, # 39 p. 6937 - 6940
反应条件
1: chloroform 2: potassium carbonate / acetonitrile / 50 °C 3: lithium hydroxide hydrate; water / acetone / 50 °C View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
反应条件
1: 88 percent / pH 2-3 2: iPr2NEt / acetonitrile / 20 h / 60 °C 3: H2 / Pd-C / ethanol / 24 h View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 185 - 186
反应条件
triethylamine in DMF (N,N-dimethyl-formamide) T=24.84°C; 14 - 20 h; Product distribution / selectivity;
参考文献
WO2005/3105 A1, ;
Page/Page column 6 ;
反应条件
sodium hydrogencarbonate in chloroform T=20°C; 72 h; Inert atmosphere;
参考文献
Main, Marcus; Snaith, John S.; Meloni, Marco M.; Jauregui, Maitey; Sykes, Daniel; Faulkner, Stephen; Kenwright, Alan M.
Chemical Communications, 2008 , # 41 p. 5212 - 5214
反应条件
in dichloromethane Ambient temperature;
参考文献
Mishra; Chatal
New Journal of Chemistry, 2001 , vol. 25, # 2 p. 336 - 339
反应条件
potassium carbonate in acetonitrile T=55 - 60°C; 4 h; Product distribution; Further Variations:Reaction partnersSolvents;
参考文献
Li, Cong; Wong, Wing-Tak
Tetrahedron Letters, 2002 , vol. 43, # 17 p. 3217 - 3220
反应条件
potassium carbonate in acetonitrile
T=55 - 60°C; 4 h;
参考文献
Li, Cong; Wong, Wing-Tak
Tetrahedron Letters, 2002 , vol. 43, # 17 p. 3217 - 3220
反应条件
formic acid in water
P=760 Torr; 30 h; Heating;
参考文献
Coates, John H.; Hadi, Dewan A.; Lincoln, Stephen F.
Australian Journal of Chemistry, 1982 , vol. 35, # 5 p. 903 - 909
参考文献
Wilson, Jennifer M.; Giordani, Federica; Farrugia, Louis J.; Barrett, Michael P.; Robins, David J.; Sutherland, Andrew
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 22 p. 3651 - 3656
