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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-苯基丙-1-胺
合成路线
（共 81 条）
72-19-5
L-苏氨酸
+
2941-20-0
1-苯基丙-1-胺
→
反应条件
1492-24-6
L-2-氨基丁酸
+
3789-59-1
(S)-(-)-1-苯丙胺
+
2941-20-0
1-苯基丙-1-胺
+
93-55-0
苯丙酮
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 28 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
2941-20-0
1-苯基丙-1-胺
+
298-12-4
乙醛酸
→
反应条件
2941-20-0
1-苯基丙-1-胺
+
93-55-0
苯丙酮
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. buffer T=37°C; pH=7.4; 12 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Jiang, Jinju; Chen, Xi; Feng, Jinhui; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 32 - 39
2941-20-0
1-苯基丙-1-胺
→
反应条件
93-55-0
苯丙酮
反应条件
iodine; mercury(II) oxide in dichloromethane T=20°C; Oxidation; 1 h;
参考文献
Orito, Kazuhiko; Hatakeyama, Takahiro; Takeo, Mitsuhiro; Uchiito, Shiho; Tokuda, Masao; Suginome, Hiroshi
Tetrahedron, 1998 , vol. 54, # 29 p. 8403 - 8410
2941-20-0
1-苯基丙-1-胺
→
反应条件
2941-20-0
1-苯基丙-1-胺
+
93-55-0
苯丙酮
反应条件
transaminase ATA-114; pyridoxal 5'-phosphate; sodium 2-oxopropanoate T=30°C; pH=7.0; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Koszelewski, Dominik; Clay, Dorina; Rozzell, David; Kroutil, Wolfgang
European Journal of Organic Chemistry, 2009 , # 14 p. 2289 - 2292
2941-20-0
1-苯基丙-1-胺
→
反应条件
3789-59-1
(S)-(-)-1-苯丙胺
+
93-55-0
苯丙酮
反应条件
transaminase ATA-117; pyridoxal 5'-phosphate; sodium 2-oxopropanoate T=30°C; pH=7.0; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Koszelewski, Dominik; Clay, Dorina; Rozzell, David; Kroutil, Wolfgang
European Journal of Organic Chemistry, 2009 , # 14 p. 2289 - 2292
72-19-5
L-苏氨酸
+
2941-20-0
1-苯基丙-1-胺
→
反应条件
1492-24-6
L-2-氨基丁酸
+
2941-20-0
1-苯基丙-1-胺
+
93-55-0
苯丙酮
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 30 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
72-19-5
L-苏氨酸
+
2941-20-0
1-苯基丙-1-胺
→
反应条件
1492-24-6
L-2-氨基丁酸
+
3789-59-1
(S)-(-)-1-苯丙胺
+
2941-20-0
1-苯基丙-1-胺
+
93-55-0
苯丙酮
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 28 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
2941-20-0
1-苯基丙-1-胺
→
反应条件
93-54-9
1-苯丙醇
+
2941-20-0
1-苯基丙-1-胺
反应条件
borane-ammonia complex; water in dimethyl sulfoxide T=30°C; pH=7; 18 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
Canadian Journal of Chemistry, , vol. 90, # 1 p. 39 - 45
485-89-2
羟辛可芬
+
2941-20-0
1-苯基丙-1-胺
→
反应条件
2387-23-7
N,N-二环己脲
+
174636-33-0
反应条件
1: With 1-hydroxybenzotriazole in tetrahydrofuran; dichloromethane; acetonitrile T=20°C; 0.666667 h; 2: With dicyclohexyl-carbodiimide in tetrahydrofuran; dichloromethane; acetonitrile T=20°C; 3: With water T=20°C; 0.5 h;
参考文献
SmithKline Beecham S.p.A.
Patent: US6355654 B1, 2002 ;
Location in patent: Page column 16 ;
2941-20-0
1-苯基丙-1-胺
+
98-88-4
苯甲酰氯
→
反应条件
57680-93-0
反应条件
sodium hydroxide
参考文献
Guijarro, David; Pablo, Oscar; Yus, Miguel
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5265 - 5270
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