6-氨基-2-甲基苯并噻唑合成路线 (共 19 条)
反应条件
hydrogenchloride; sodium nitrite Behandeln der Reaktionsloesung mit SO2 und CuCl2 enthaltender wss. Essigsaeure;
参考文献
Libeer et al.
Bulletin des Societes Chimiques Belges, 1971 , vol. 80, p. 43,47
反应条件
sodium tetrahydroborate; sulfuric acid in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Hrobarik, Peter; Sigmundova, Ivica; Zahradnik, Pavol
Synthesis, 2005 , # 4 art. no. P11804SS, p. 600 - 604
反应条件
1: With hydrogenchloride; sodium nitrite 0.5 h; cooling; 2: With potassium iodide in water T=40°C; 0.166667 h;
参考文献
Helvetica Chimica Acta, , vol. 88, # 5 p. 1135 - 1143
反应条件
N,N-dichlorourea in acetic acid
参考文献
Grandolini,G. et al.
Journal of Heterocyclic Chemistry, 1966 , vol. 3, p. 299 - 301
反应条件
1: Br2, NH4Br / methanol
2: aq. Na2S
View Scheme
参考文献
Fridman,S.G.; Golub,D.K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, p. 481 - 487
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, p. 713 - 721
参考文献
Dzyubenko, V. G.; Abramenko, P. I.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 750 - 753
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 4 p. 831 - 835
反应条件
1: CHCl3; H2O
2: NaN3 / H2O
View Scheme
参考文献
Kudrenko,V.A. et al.
Sov. Prog. Chem. (Engl. Transl.), 1975 , vol. 41, # 7 p. 764 - 767,87 - 89
反应条件
bromine; NH4Br in methanol
参考文献
Fridman,S.G.; Golub,D.K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, p. 481 - 487
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, p. 713 - 721
参考文献
Meheux,P. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1972 , vol. 275, p. 669 - 672