4-硝基-4'-甲氧基偶氮苯合成路线 (共 18 条)
反应条件
1: 4-(4'-hydroxyphenylazo)nitrobenzene With potassium hydroxide in dichloromethane; water 0.166667 h; 2: methyl iodide in dichloromethane 40 h; RefluxInert atmosphere;
参考文献
Raymo, Francisco M.; Tomasulo, Massimiliano
Patent: US2009/258429 A1, 2009 ;
Location in patent: Page/Page column 8 ;
反应条件
Na[B(3,5-(CF3)2C6H3)4] in dichloromethane; water 48 h; Ambient temperature;
参考文献
Iwamoto, Hidetoshi; Yoshimura, Masaji; Sonoda, Takaaki; Kobayashi, Hiroshi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 3 p. 796 - 801
反应条件
in acetonitrile 7 h; Ambient temperature;
参考文献
Neumann, Wilhelm P.; Wicenec, Christian
Chemische Berichte, 1991 , vol. 124, # 10 p. 2297 - 2301
反应条件
1: 1.) NaNO2, 20percent aq. HCl, 2.) 5percent aq. NaOH / 1.) 0 deg C 2: MeONa / methanol / 3 h / Heating View Scheme
参考文献
Nesterowicz, Marianna; Korewa, Ryszard
Polish Journal of Chemistry, 1981 , vol. 55, # 5 p. 1085 - 1092
反应条件
1: 1.) NaNO2, 20percent aq. HCl, 2.) 5percent aq. NaOH / 1.) 0 deg C 2: MeONa / methanol / 3 h / Heating View Scheme
参考文献
Nesterowicz, Marianna; Korewa, Ryszard
Polish Journal of Chemistry, 1981 , vol. 55, # 5 p. 1085 - 1092
参考文献
Weizmann
Transactions of the Faraday Society, 1940 , vol. 36, p. 978,981
反应条件
perchloric acid in isopropyl alcohol; acetonitrile T=25°C; pH=2; 0.833333 h; Inert atmosphereIrradiation;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 318, # 1-2 p. 75 - 84
反应条件
perchloric acid in isopropyl alcohol; acetonitrile T=25°C; pH=2; 0.833333 h; Inert atmosphereIrradiation;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 318, # 1-2 p. 75 - 84
参考文献
Schmidt,O.
Chemische Berichte, 1905 , vol. 38, p. 3209,3210
反应条件
nitric acid Salz entsteht;
参考文献
Schmidt,O.
Chemische Berichte, 1905 , vol. 38, p. 3203,3208