5-氯-1-碘-2-甲基-3-硝基苯合成路线 (共 2 条)
反应条件
N-iodo-succinimide; sulfuric acid T=0°C; 1 h; Product distribution; Further Variations:TemperaturesReagentsreaction times;
参考文献
Katayama; Ae; Nagata
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3474 - 3483
反应条件
1: With acetic acid; tin(ll) chloride T=20°C; 1 h; 2: With sodium hydroxide in diethyl ether; water T=0°C;
参考文献
EXELIXIS, INC.
Patent: WO2005/117909 A2, 2005 ;
Location in patent: Page/Page column 113 ;
WO 2005/117909 A2