1-[(4-甲基苯基)氨基]蒽醌合成路线 （共 11 条）
反应条件
sodium hydroxide; hydrazine hydrate in ethylene glycol T=100°C; 3 h;
参考文献
Kazankov, M. V.; Ginodman, L. G.; Mustafina, M. Ya.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 1 p. 139 - 144
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 1 p. 153 - 158
反应条件
sodium hydroxide; hydrazine hydrate in ethylene glycol 1) 100 deg C, 4 h, 2) 160 deg C, 2 h;
参考文献
Kazankov, M. V.; Ginodman, L. G.; Mustafina, M. Ya.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 526 - 533
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 597 - 606
反应条件
1: 98 percent / conc. H2SO4, sodium m-nitrobenzenesulfonate / 3 h / Ambient temperature 2: 50 percent / NH2NH2*H2O, NaOH / ethane-1,2-diol / 1) 100 deg C, 4 h, 2) 160 deg C, 2 h View Scheme
参考文献
Kazankov, M. V.; Ginodman, L. G.; Mustafina, M. Ya.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 526 - 533
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 597 - 606
反应条件
1: 92 percent / conc. H2SO4 / 0.07 h / Ambient temperature 2: 50 percent / NH2NH2*H2O, NaOH / ethane-1,2-diol / 1) 100 deg C, 4 h, 2) 160 deg C, 2 h View Scheme
参考文献
Kazankov, M. V.; Ginodman, L. G.; Mustafina, M. Ya.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 526 - 533
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 597 - 606
反应条件
boric acid T=130°C; Behandeln des Reaktionsprodukts mit wss.-methanol. Alkalilauge;
参考文献
Zahn; Koch
Chemische Berichte, 1938 , vol. 71, p. 172,178
参考文献
Bayer and Co.
Patent: DE175024 ;
反应条件
1: chlorobenzene; nickel /kieselguhr / 80 - 120 °C / 51485.6 Torr / Hydrogenation 2: boric acid / 130 °C / Behandeln des Reaktionsprodukts mit wss.-methanol. Alkalilauge View Scheme
参考文献
Zahn; Koch
Chemische Berichte, 1938 , vol. 71, p. 172,178
参考文献
Bayer and Co.
Patent: DE115048 ;
参考文献
Putschkow
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3058,3064; engl. Ausg. S. 3024, 3028
反应条件
T=180°C; unter Druck;
参考文献
Bayer and Co.
Patent: DE175024 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 8, p. 284
