1-(4-羟苯基)哌嗪二氰溴化物合成路线 (共 61 条)
反应条件
boron trifluoride in neat (no solvent) T=25°C; 0.0833333 h; further solvents; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 106, # 18 p. 5284 - 5290
反应条件
aluminium trichloride in nitromethane T=25°C; 0.0833333 h; further solents; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 106, # 18 p. 5284 - 5290
反应条件
aluminium trichloride in nitromethane T=25°C; 0.166667 h; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 106, # 18 p. 5284 - 5290
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; [copperl(II)(1,1,1,5,5,5-hexafluoroacetylacetonate)2] monohydrate; palladium diacetate in tert-butyl alcohol T=100°C; 3 h; Inert atmosphere;
参考文献
Nakao, Yoshiaki; Takeda, Masahide; Matsumoto, Takuya; Hiyama, Tamejiro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 26 p. 4447 - 4450
反应条件
4-Methyl-1,1,3,3-tetrabutylguanidine T=180°C; 4.5 h;
参考文献
Barcelo, Gerard; Grenouillat, Denis; Senet, Jean-Pierre; Sennyey, Gerard
Tetrahedron, 1990 , vol. 46, # 6 p. 1839 - 1848
反应条件
1: 75 percent / PCC, HOAc, Celite, molecular sieve 4A / CH2Cl2 View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 127 - 132
反应条件
thionyl chloride 50 h; Reflux;
参考文献
Bridoux, Alexandre; Khan, Riaz A.; Chen, Celei; Cheve, Gwenael; Cui, Huadong; Dyskin, Evgeny; Yasri, Aziz; Mousa, Shaker A.
Journal of Enzyme Inhibition and Medicinal Chemistry, 2011 , vol. 26, # 6 p. 871 - 882
反应条件
aluminium trichloride in nitromethane time, solvent and temperature dependence of isomerization; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 106, # 18 p. 5284 - 5290
反应条件
phosphoric acid T=95°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 15, p. 820,822
Chem.Abstr., , p. 732
反应条件
ethanol; platinum Hydrogenation;
参考文献
Journal of the Indian Chemical Society, , vol. 36, p. 659,665