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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2946-02-3
合成路线
（共 7 条）
2816-87-7
+
108-24-7
乙酸酐
→
反应条件
2946-02-3
反应条件
pyridine
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
18549-40-1
1,2-O-异亚丙基-D-呋喃葡萄糖
→
反应条件
2946-02-3
反应条件
1: 1.) Bu2SnO / 1.) MeOH, reflux, 3 h, 2.) dioxane, from 5 deg C to 10 deg C, 1 h 2: 96 percent / pyridine View Scheme
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
2946-02-3
→
反应条件
32953-62-1
反应条件
potassium iodide in acetonitrile T=140°C; 6 h;
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
2946-02-3
→
反应条件
32953-62-1
+
113119-58-7
反应条件
azobisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=110°C; 3 h; Title compound not separated from byproducts;
参考文献
Tsuda, Yoshisuke; Kanemitsu, Kimihiro; Kakimoto, Kyoko; Kikuchi, Tohru
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 5 p. 2148 - 2150
2946-02-3
→
反应条件
反应条件
1,1,1,2,2,2-hexabutyl-distannane in benzene T=10 - 15°C; 4 h; Irradiation; Further byproducts given;
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
2946-02-3
→
反应条件
32953-62-1
+
113119-63-4
+
113119-58-7
反应条件
1,1,1,2,2,2-hexabutyl-distannane in benzene T=10 - 15°C; 4 h; Irradiation; Further byproducts given;
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
2946-02-3
→
反应条件
反应条件
1,1,1,2,2,2-hexabutyl-distannane in benzene 4 h; Irradiation; Further byproducts given;
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
