反应条件
1: Escherichia coli JM109 (pDTG601A) 2: TsOH / acetone / Ambient temperature 3: NaIO4 / Ambient temperature 4: 1.) Pd(PPh3)4, aq. NaCO3; 2.) Mo(CO)6 / 1.) PhH, reflux; 2.) PhH, MeCN, H2O, reflux, 10 h 5: 80 percent / NaBH4, CeCl3 / methanol / 0 °C 6: 65 percent / Bu3P, DEAD / tetrahydrofuran / Ambient temperature 7: Dowex 50X8-100 / methanol / Ambient temperature 8: pyridine, DMAP / Ambient temperature 9: 40 percent / Tf2O, DMAP / CH2Cl2 / 0 °C 10: Amberlyst A21 / methanol / Ambient temperature 11: LiCl / dimethylformamide / 120 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 16 p. 3077 - 3080
