1-(3-溴苯基)-1H-吡唑合成路线 （共 4 条）
反应条件
copper(l) iodide; (1S,2S)-1,2-diaminocyclohexane; potassium carbonate in 1,4-dioxane 19 h; Reflux;
参考文献
Universal Display Corporation; Beers, Scott; Xia, Chuanjun; Brooks, Jason; Kottas, Gregg
Patent: EP2574613 A1, 2013 ;
Location in patent: Paragraph 0144 ;
反应条件
1: [3,2-c]pyrazole With sodium hydride in N,N-dimethyl-formamide T=20°C; 0.5 h; 2: 3-fluoro-1-bromobenzene in N,N-dimethyl-formamide T=130°C; 2 h;
参考文献
MSD OSS B.V.; HUISMAN, Ines; VAN DER STELT, Marcelis; WIEDENHOF, Wouter; BAKER-GLENN, Charles, Anthony, Graham; BLACKABY, Wesley, Peter; TRIVEDI, Naimisha
Patent: WO2013/41457 A1, 2013 ;
Location in patent: Page/Page column 23 ;
反应条件
copper(I) oxide; sodium t-butanolate in 1-methyl-pyrrolidin-2-one T=100°C; 15 h; Microwave irradiation;
参考文献
Boswell, Mikki G.; Yeung, Fanny G.; Wolf, Christian
Synlett, 2012 , vol. 23, # 8 p. 1240 - 1244
反应条件
hydrogenchloride in ethanol; water Heating;
参考文献
Magnetic Resonance in Chemistry, , vol. 49, # 8 p. 537 - 542
